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Summary - Low temperature work and reduced scale apparatus as used by a modern organic chemist in separation processes.
Summary - Low temperature work and reduced scale apparatus as used by a modern organic chemist in separation processes.
| Module code and title: | S344, Organic chemistry: a synthesis approach |
|---|---|
| Item code: | S344; VCR6 |
| First transmission date: | 1989 |
| Published: | 1989 |
| Rights Statement: | |
| Restrictions on use: | |
| Duration: | 00:25:00 |
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| Producer: | Ted Smith |
| Contributor: | Michael Gagan |
| Publisher: | BBC Open University |
| Keyword(s): | Buchner flask; Butyl; Lithium; Reagent; Recrystallisation; Wilstatter nail |
| Footage description: | Footage - Robert Robertson's paper on annulation reaction. Paper on synthesis of trichodermin (0'22"-1'34") - B10 apparatus. Small scale recrystallisation apparatus. Buchner apparatus (1'43"-3'22") - Wilstatter nail (4'43"-5'39") - Diagram of apparatus without any joints (5'55"-6'11") - Bulb to bulb distillation apparatus. Kugelrohr (6'21"-7'24") - Reagents in fume cupboard (7'43"-7'55") - Diagram of Grignard reaction. Grignard reaction apparatus (8'20"-10'40") - Solution transfer of a reagent using nitrogen pressure (10'58"-14'00") - Salt ice bath. Acetone & dry ice coolant (15'10"-16'15") - Butyl lithium added to a solution of diphenyl acetic acid to generate the dianion (16'33"-19'00"). |
| Master spool number: | HOU6342 |
| Production number: | FOUS580L |
| Videofinder number: | 3024 |
| Available to public: | no |
