Available online
Description
The theoretical basis of nuclear magnetic resonance (NMR) and its measurement by continuous wave and pulsed Fourier transform techniques.
The theoretical basis of nuclear magnetic resonance (NMR) and its measurement by continuous wave and pulsed Fourier transform techniques.
| Module code and title: | S304, The nature of chemistry |
|---|---|
| Item code: | S304; 08 |
| First transmission date: | 07-06-1976 |
| Published: | 1976 |
| Rights Statement: | |
| Restrictions on use: | |
| Duration: | 00:24:00 |
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| Producer: | David Jackson |
| Contributors: | Alan Bassindale; Joan Mason |
| Publisher: | BBC Open University |
| Keyword(s): | Absorbtion peaks; Fourier transform techniques; Nuclear magnetic resonance; Proton spectra; Spin coupling |
| Footage description: | Footage - Proton decoupled carbon 13 NMR spectrum (0'01"-1'24") - Graphic of NMR (1'37"-2'16") - Graphic of applied field (2'49"-3'36") - Proton spectrum of chloroform (3'37"-3'49") - Equation of resonance frequency (4'28"-5'12") - Molecular model of 2-propenol. Carbon 13 NMR spectrum of 2-propenol (5'56"-6'52") - Proton instrument (6'59"-7'06") - Continuous wave field sweep spectrometer. Sample placed between poles of magnet. Graphic of instrument (7'20"-9'31") - Caffeine dissolved in deutero chloroform put into spectrometer. Spectrum of caffeine (9'55"-10'35") - Spinning solution of caffeine. NMR spectrum of caffeine (10'48"-11'28") - Resonance frequency signal (13'22"-13'45") - Free Induction Decay (FID) pattern (14'58"-15'15") - FID pattern & spectrum (16'01"-16'33") - Double irradiation spectra. Molecular model of dichloroacetaldehyde. Proton spectrum. Spectrum of decoupled protons (16'52"-19'32") - Molecular model and spectrum of 2-propenol (19'36"-21'56"). Carbon spectrum. 2-propanol spectrum (22'12"-22'30") - Molecular model and off-resonant spectrum of 2-propanol (22'42"-23'30") - Proton spectrum of cholesteryl acetate. Carbon spectrum with coupling present of cholesteryl acetate (23'40"-24'12"). |
| Master spool number: | 6HT/71972 |
| Production number: | 00525_1198 |
| Videofinder number: | 863 |
| Available to public: | no |
